Test Sample Chromatograms
Test sample chromatograms
Figure
HP 5890 Test Sample Operating
Conditions
Detector Type ECDw/MUG | FLOW RATES |
|
| ||||
Temp 300 DEGREES C | Carrier (He) | 15 +/• 1 | ml/min | ||||
Inlet Type Split only or | Hydrogen | N/A | ml/min | ||||
splitless |
| Air | N/A | ml/min | |||
Temp 200 DEGREES C |
| Makeup (N2) | 60 +/• 2 | ml/min | |||
Operating Mode Split(Purge on) | Split Vent | 60 +/• 2 | ml/min | ||||
Purge Time On | 0 |
| min | Septum Purge | 5 +/• 1 | ml/min | |
Purge Time Off | 0 |
| min |
|
|
| |
Oven Temp Isothermal |
|
|
|
| |||
Init Temp | 170 | DEGREES C |
|
|
| ||
Init Time | N/A | min | SAMPLE: |
|
| ||
Ramp |
|
|
|
|
|
| |
Rate |
| 0 |
|
| Type ECD Sample |
| |
Fin Temp |
|
|
|
| Inj Volume | 1 ¿l |
|
Fin Time |
|
|
|
| Part No. 18713•60040 |
| |
Range 0 |
|
|
|
| Composition 33 pg/¿l (0.033 | ||
|
|
|
|
| ppm (W/V)) each: lindane |
| |
COLUMN: |
|
|
|
| and aldrin in isooctane |
| |
Part No. | 19095S(#100) |
|
|
| |||
Dimensions |
| 530¿ MID; 5 m |
|
|
| ||
Sta Phase | Methyl Silicone |
|
|
| |||
.37
.43
1.13 LINDANE
2.64ALDRIN
ST
232