Test Sample Chromatograms
Test sample chromatograms
Figure
HP 5890 Test Sample Operating
Conditions
Detector Type | FIDw/MUG |
| FLOW RATES |
|
| |||||
| Temp 250 DEGREES C |
| Carrier (He) | 15 +/• 1 | ml/min | |||||
Inlet Type Ded |
| Hydrogen | 30 +/• 1 | ml/min | ||||||
Oven Track |
|
| On |
|
| Air | 400 +/• 20 | ml/min | ||
| Temp N/A |
| C | Makeup (N2) | 20 +/• 1 | ml/min | ||||
Operating Mode |
| N/A |
| Split Vent | N/A | ml/min | ||||
Purge Time On |
| N/A | min | Septum Purge | 5 +/• 1 | ml/min | ||||
Purge Time Off |
| N/A | min |
|
|
| ||||
Oven Temp Temp Programmed (1 |
|
|
| |||||||
ramp) |
|
|
|
|
|
|
|
|
|
|
Init Temp | 60 | DEGREES C |
|
|
| |||||
Init Time | 0.5 | min |
|
|
|
| ||||
Ramp |
|
|
|
|
|
|
| SAMPLE: |
|
|
Rate |
|
| 20 |
|
|
|
|
| ||
|
|
|
|
| Type FID Sample |
| ||||
Fin Temp |
|
| 185 |
|
|
|
| |||
Fin Time |
|
| 1 |
|
|
| Inj Volume | 1 ¿l |
| |
Flow Param (EPP) |
|
| Part No. 18710•60170 |
| ||||||
|
| Composition 0.03%(V/V)each: | ||||||||
Constant Flow | Off |
| ||||||||
| C14,C15, and C16 normal paraffin | |||||||||
Range | 4 |
|
|
|
|
|
| |||
|
|
|
|
|
| hydrocarbons in hexane. |
| |||
|
|
|
|
|
|
|
|
| ||
COLUMN: |
|
|
|
|
|
|
|
|
|
|
Part No. |
| 19095(#100) |
|
|
|
| ||||
Dimensions |
|
| 530¿ MID; 5 M |
|
|
| ||||
Sta Phase | Methyl Silicone |
| .112 |
| ||||||
|
|
|
|
|
|
| START |
| ||
|
|
|
|
|
|
|
|
| .331 | .267 |
4.743 C14
5.398 C15
6.322 C16
229