Test Sample Chromatograms
Test sample chromatograms
Figure
HP 5890 Test Sample Operating
Conditions
Detector | Type FPD |
| |
| Temp | 200 | DEGREES C |
Inlet Type PACKED OR PURGED | |||
| PACKED |
| |
| Temp | 200 | DEGREES C |
Operating Mode | N/A |
| |
Purge Time On | N/A | min | |
Purge Time Off | N/A | min | |
Oven Temp Programmed (1 ramp) |
| ||
Init Temp | 110 | DEGREES C | |
Init Time | 0 | min |
|
Ramp Rate | ___10 |
|
|
Fin Temp | __170 |
|
|
Fin Time | ____3 |
|
|
Range 5 |
|
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|
COLUMN: |
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|
|
Part No. | 19095S•100 |
|
|
Dimensions | 5 M Length, 530 ¿ | ID | |
Sta Phase Methyl Silicone
FLOW RATES (FPD AIR MODE FLOWS) |
| ||
Carrier (N2) | 20 | +/• 1 | ml/min |
Hydrogen | 75 | +/• 2 | ml/min |
Air | 100 +/• 3 | ml/min | |
Makeup (N2) |
| 0 | ml/min |
Split Vent |
| N/A | ml/min |
Septum Purge |
| 1•2 | ml/min |
SAMPLE:
Type FPD Sample
Inj Volume 1 ¿l Part No. 19395•60580 COMPOSITION: 20 ng/¿l (20.0 ppm W/V) each of
START | IF | Sulfer | START | IF | Phospho- |
| .07 |
| .07 | ||
|
| Filter |
| .44 | rus |
|
|
|
| ||
| 1.73 |
|
|
| Filter |
| 2.11 | DODECANETHIOL | 2.10 DODECANETHIOL | ||
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| ||||
|
| 2.46 |
| ||
|
|
|
| TRIBUTYLPHOS- | |
| 3.16 | TRIBUTYLPHOSPHATE |
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| |
|
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| 3.16 | ||
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|
|
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| PHATE |
ZE | ZE |
|
FPD Packed Column Inlet
237