Test Sample Chromatograms
Test sample chromatograms
Figure
HP 5890 Test Sample Operating
Conditions
Detector | Type FPD |
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| Temp 200 DEGREES C |
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Inlet Type DED |
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Oven Track |
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| On |
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| Temp N/A | DEGREES C |
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Operating | Mode |
| N/A |
|
Purge Time On |
| N/A | min | |
Purge Time Off |
| N/A | min | |
Oven Temp Programmed (1 ramp) |
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Init Temp | 90 | DEGREES C | ||
Init Time | 1.0 | min |
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Ramp |
| (1) | (2) |
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Rate |
| 20 | 10 |
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Fin Temp | 110 | 170 |
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Fin Time | 0 | 3 |
| |
Flow Param (EPP) |
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| ||
Constant Flow | Off |
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Range 5 |
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COLUMN: |
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Part No. |
| 19095S•100 |
| |
Dimensions |
| 5 M Length, 530 ¿ | ID | |
Sta Phase Methyl Silicone
FLOW RATES (FPD AIR MODE FLOWS) |
| |||
Carrier (N2) |
| 20 +/• 1 | ml/min | |
Hydrogen |
| 75 +/• 2 | ml/min | |
Air |
|
| 100 +/• 3 | ml/min |
Makeup (N2) |
| 0 | ml/min | |
Split Vent |
| N/A | ml/min | |
Septum Purge |
| 5 +/• 1 | ml/min | |
SAMPLE: |
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Type | FPD Sample |
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Inj Volume | 1 | ¿l |
| |
Part No. 19395•60580 |
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COMPOSITION: 20 ng/¿L |
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(20.0 ppm W/V) each of |
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and |
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tributylphosphate in isooctane
START .13 | START | .13 |
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|
| ||
| Sulfer | .49 | Phosphorus |
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| ||
1.91 | Filter | 1.45 | Filter |
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|
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4.06 DODECANETHIOL
| 4.08 | |
| 4.57 | |
3.35 | TRIBUTYLPHOS- | |
5.37 | ||
| ||
| PHATE | |
IF | IF | |
|
FPD
239