Test Sample Chromatograms
Test sample chromatograms
Figure
HP 5890 Test Sample Operating
Conditions
Detector | Type FPD |
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| |
| Temp 200 DEGREES C | |||
Inlet Type SPLIT ONLY OR |
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SPLIT/SPLITLESS |
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| |
| Temp 200 | DEGREES C | ||
Operating | Mode |
| SPLIT(PURGE ON) | |
Purge Time On |
| 0 | min | |
Purge Time Off |
| 0 | min | |
Oven Temp Programmed (1 ramp) | ||||
Init Temp |
| 110 | DEGREES C | |
Init Time |
| 0 | min | |
Ramp Rate | ___10 |
| ||
Fin Temp | _ 170 |
| ||
Fin Time | ____3 |
| ||
Range 5 |
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COLUMN: |
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|
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Part No. |
| 19095Z•121 |
| |
Dimensions |
| 5 M Length, 530 ¿ ID | ||
Sta Phase Methyl Silicone
FLOW RATES (FPD AIR MODE FLOWS) |
| ||
Carrier (N2) | 20 | +/• 1 | ml/min |
Hydrogen | 75 | +/• 2 | ml/min |
Air | 100 +/• 3 | ml/min | |
Makeup (N2) |
| 0 | ml/min |
Split Vent | 200 | +/• 20 | ml/min |
Septum Purge | 5 +/• 1 | ml/min | |
SAMPLE:
Type FPD Sample
Inj Volume 2 ¿l Part No. 19305•60580 COMPOSITION: 20 ng/¿l (20.0 ppm W/V) each of
IF
START .11
.84Sulfer Filter
START
.11
.71Phosphorus Filter
2.88 DODECANETHIOL | DODECANETHIOL | |
2.88 | ||
3.70 TRIBUTYLPHOS- | 3.70 | |
PHATE | ||
TRIBUTYLPHOS- | ||
| ||
| PHATE | |
ZE |
| |
ZE |
|
FPD Split Mode Capillary Inlet
238