Test Sample Chromatograms

Test sample chromatograms

Figure 10-10.

HP 5890 Test Sample Operating

Conditions

Detector Type NPD w/MUG) Temp 220 DEGREES C

Inlet Type Ded On-Col Cap

Oven Track

 

 

On

 

 

Temp N/A

C

 

 

 

 

 

Operating Mode N/A

 

 

Purge Time On

 

 

 

 

min

Purge Time Off

 

 

 

 

min

Oven Isothermal

 

 

 

 

 

Init Temp

170

DEGREES C

Init Time

5.0

 

min

Ramp

 

 

 

 

 

 

Rate

 

0

 

 

 

 

Fin Temp

 

 

 

 

 

Fin Time

 

 

 

 

 

Flow Param (EPP)

 

 

Constant Flow

Off

Range 0

 

 

 

 

 

 

COLUMN:

 

 

 

 

 

 

Part No.

19095S(#100)

Dimensions

 

530¿ MID; 5 M

Sta Phase

Methyl Silicone

START

<P

FLOW RATES

 

 

 

Carrier (He)

15 +/• 1

ml/min

Hydrogen

4

+/• 1

ml/min

Air

90

+/• 10

ml/min

Makeup (He)

10+/•1

ml/min

Split Vent

 

N/A

ml/min

Septum Purge

 

5+/•1

ml/min

SAMPLE:

Type NP-FID Sample Inj Volume 3 ¿l Part No. 18789•60060 Composition 0.65 ppm azobenzene, 100 ppm octadecane, 1.0 ppm malathion in isoioctane

IF

IF

AZOBENZENE

.896

IF

1.966 OCTADECANE

3.356 MALATHION

ST

NPD-On-Column Capillary Inlet

234