Index
S
septum, changing packed column inlet, 159 split/splitless capillary inlet, 163
septum purge, packed inlet, 105
septum purged packed column inlet, 103
setpoint protection, 38
setpoints displaying, 33 entering, 34 ranges, 46
solvent effect, 114
solvent purity, 118
spiking problems, 206
split capillary inlet inserts, 27
split ratio, 112
split sampling, 111
split/splitless capillary inlet, 107, 163 cleaning, 168
insert care, 164 leaks, 165
split/splitless inlet inserts, 27
split/splitless sampling, injection technique, 121
splitless sampling, 114 inlet insert purge, 118 inlet temperature, 117 sample requirements, 117 solvent purity, 118
sub•ambientoven control, 47
T
TCD, 192 cleaning, 192
on•columntest chromatogram, 235 split inlet test chromatogram, 233 test chromatogram, 228
temperature control, 44
temperature programming, oven, 49
test chromatograms, 224
troubleshooting, 202
troubleshooting electronic pressure control, 218
V
valves
locating leaks, 216 troubleshooting, 214
W
wipe test, ECD, 192
244