Test Sample Chromatograms
Test sample chromatograms
Figure
HP 5890 Test Sample Operating
Conditions
Detector Type | TCDw/MUG | FLOW RATES |
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| Temp 300 DEGREES C | Carrier (He) | 15 +/• 1 |
| ml/min | ||||||
Inlet Type Split only or | Hydrogen | N/A |
| ml/min | |||||||
| split/splitless | Air |
| N/A4 |
| ml/min | |||||
Temp | 250 DEG C |
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| Makeup (He) | 10 +/• 1 |
| ml/min | ||
Operating Mode Split(Purge on) | Split Vent | 200 +/• 10 |
| ml/min | |||||||
Purge Time On | 0 |
| min | Septum Purge | 5 +/• 1 |
| ml/min | ||||
Purge Time Off | 0 |
| min | Reference (He)37 +/• 1 |
| ml/min | |||||
Oven Temp Programmed |
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Init Temp | 100 | DEGREES C |
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Init Time | 1 | min |
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Ramp |
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Rate |
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| 10 |
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| SAMPLE: |
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Fin Temp |
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| 150 |
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| Type | Capillary |
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Fin Time |
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| 2 |
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| Inj Volume | 1 ¿l |
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Range | 0 |
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| Part No. 18740•60900 |
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| Composition See Split/FID |
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COLUMN: |
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Part No. | 19095Z(121) |
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Dimensions |
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| 530¿ MID; 5 M |
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Sta Phase | Methyl Silicone |
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| START | .11 |
| .15 | .42 | |
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| .25 |
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| C9 |
3.64
4.78
ST
3.85
4.45
6.48
C16
233