Test Sample Chromatograms
Test sample chromatograms
Figure
HP 5890 Test Sample Operating
Conditions
Detector Type | TCDw/MUG | |||||
| Temp 300 DEGREES C | |||||
Inlet Type Ded |
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Oven Track |
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| On |
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| Temp N/A | C | ||||
Operating Mode |
| N/A |
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Purge Time On |
| N/A | min | |||
Purge Time Off |
| N/A | min | |||
Oven Temp Programmed (1 ramp) | ||||||
Init Temp | 60 | DEGREES C | ||||
Init Time | 0.5 | min | ||||
Ramp |
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Rate |
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| 20 |
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Fin Temp |
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| 180 |
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Fin Time |
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| 1 |
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Flow Param (EPP) |
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Constant Flow | Off | |||||
Range | 0 |
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COLUMN: |
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Part No. |
| 19095S(#100) | ||||
Dimensions |
|
| 530¿ MID; 5 M | |||
Sta Phase | Methyl Silicone | |||||
FLOW RATES |
|
|
Carrier (He) | 20 +/• 1 | ml/min |
Hydrogen | N/A | ml/min |
Air | N/A | ml/min |
Makeup (He) | 5+/•1 | ml/min |
Split Vent | N/A | ml/min |
Septum Purge | 5+/•1 | ml/min |
Reference (He) 37+/•1 | ml/min | |
SAMPLE:
Type FID Sample
Inj Volume 3 ¿l Part No. 18710•60170 Composition 0.03%(V/V)each C14,C15,C16 normal paraffin hydrocarbons in hexane.
4.23 C14
4.82 C15
5.38 C16
235