Test Sample Chromatograms

Test sample chromatograms

Figure 10-6.

HP 5890 Test Sample Operating Conditions

Detector Type

FIDw/MUG

 

Temp 250 DEGREES C

Inlet Type SPLIT ONLY OR

SPLIT/SPLITLESS Temp

200 DEG C

Operating Mode SPLIT(PURGE ON)

Purge Time On

0

 

 

min

Purge Time Off

0

 

 

min

Oven Temp Programmed (1 ramp)

Init Temp

 

100

DEGREES C

Init Time

 

0

 

min

Ramp

 

 

 

 

 

 

 

Rate

 

 

20

 

 

 

Fin Temp

 

 

180

 

 

 

Fin Time

 

1

 

 

 

Range

7

 

 

 

 

 

 

COLUMN:

 

 

 

 

 

 

 

Part No.

 

19095Z•121

 

Dimensions

 

 

530¿ ; 10 M

Sta Phase

Methyl Silicone

START

2.21 2.35

2.81

FLOW RATES

 

 

 

Carrier (He)

15

+/• 1

ml/min

Hydrogen

30

+/• 1

ml/min

Air

400

+/• 20

ml/min

Makeup (N2)

20

+/• 1

ml/min

Split Vent

200

+/• 20

ml/min

Septum Purge

5 +/• 1

ml/min

SAMPLE:

Type Capillary Sample Inj Volume 1 ¿l Part No. 18740•60900 Composition: Soln of 0.1%(w/w) n-nonane,n-hexadecane and 0.1% (w/w)each of 1-octanol,nonanol, n-undecane,naphthalene,2-deca- none,n-dadecane,n-tridecane,

1-pentadecane in tetradecane.

.40 C9

2.64

3.67 C16

ST

FID-Split Mode Capillary Inlet

230