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Teledyne 6600 Oil in Water Sample Conditioning System Operation, Part III: Sample System, Model

Models: 6600

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Part III: Oil in Water

OPERATING INSTRUCTIONS

Model 6600

Oil in Water

Sample Conditioning

System Operation

Part III: Sample System

X-Proof

Part Number D-

6600 - GP, Rack, Panel (Integral or Remote) 6600Z - GP, Bulkhead (Z-Purged in Div II areas) (Integral or Remote)

6600X - (X-Proof, 1,1,B, C, D) (Integral or Remote)

Teledyne Analytical Instruments

Part III: i

Page 87

Image 87

Teledyne 6600 Oil in Water Sample Conditioning System Operation, Part III: Sample System, Model, Operating Instructions

Contents

Model Oil in Water AnalyzerOPERATING INSTRUCTIONS DANGERCopyright 1999 Teledyne Analytical Instruments WarrantyModel Teledyne Analytical InstrumentsPart II: Analysis Section Table of ContentsPart I: Control Section PartTeledyne Analytical Instruments Modelof the Control/Analysis Unit ModelOil in Water Analyzer Part I: Control SectionModel 6600 Oil in Water Analyzer Table of ContentsInstallation ii: PartA Appendix 4 MaintenancePart I: Part I: Control Sectioniv: Part Model 6600 Oil in Water AnalyzerTeledyne Analytical Instruments Part I: Control Section Introduction1.1Overview Oil in Water AnalyzerModel 1.3Main Features of the Analyzer1.4Operator Interface 1 IntroductionPart I: Control Section 1.4.1 UP/DOWN Switch1.4.2 ESCAPE/ENTER Switch Oil in Water AnalyzerTeledyne Analytical Instruments 1 IntroductionModel 1-4:PartFigure 1-2:Model 6600 Interface Panel Oil in Water AnalyzerPart I: Control Section Teledyne Analytical Instruments• Analog Outputs 1.5Control Section Interface Panel1 Introduction ModelPart I: Installation2.1Unpacking the Control/Analysis Unit 2.2Electrical ConnectionsModel 2 Installation115VAC 2-2:PartExamples Part I:Oil in Water Analyzer Part I: Control SectionTeledyne Analytical Instruments 2 Installation2-4:Part ModelOil in Water Analyzer Alarm RelaysThe connectors are Part I:Digital Remote Cal Inputs 2 Installation2-6:Part ModelPart I: Control Section Table 2-3: RS-232SignalsPart I: Oil in Water Analyzer2-8:Part 2 InstallationCommand SettingPart I: Control Section 2.3Testing the SystemPart I: Oil in Water AnalyzerTeledyne Analytical Instruments 2 Installation2-10:Part ModelPart I Operation3.2Using the Controls 3.1Introduction3.2.1Mode/Function Selection 3-2Part3 Operation ModelTeledyne Analytical Instruments Part IOil in Water Analyzer OperationModel 3.3The System Function3-4Part 3 OperationOperation 3.3.1 Setting up an AUTO-CALPart I Oil in Water Analyzer3 Operation 3.3.2 Password Protection3.3.2.1EnteringthePassword 3-6PartOperation 3.3.2.2Installing or Changing the PasswordPart I Oil in Water Analyzer3.3.3 Logging Out 3-8Part3 Operation ModelOperation 3.3.4 System Self-DiagnosticTestPart I Oil in Water Analyzer3.3.5 The Model Screen 3-10Part3 Operation ModelOil in Water Analyzer 3.3.7 Digital Filter SetupSetting Part IModel 3.3.8 Homogenizer Function Setup3-12Part 3 OperationPart I 3.3.9Hold/Track SetupAUTOCAL HMGNZR TRACK CAL-HOLDER-TIMERMORE or AUTOCAL HMGNZR HOLD CAL-HOLD-TIMERMORE3-14Part 3.3.10 Calibration/Hold Timer SetupAUTOCAL HMGNZR TRACK CAL-HOLD-TIMERMORE or AUTOCAL HMGNZR HOLD CAL-HOLD-TIMERMOREPart I AUTOCAL HMGNZR TRACK CAL-HOLD-TIMERMORE orAUTOCAL HMGNZR HOLD CAL-HOLD-TIMERMORE Adjust 4 maModel 3.4The Zero and Span Functions3-16Part 3 OperationOperation 3.4.1.1Auto Mode ZeroingPart I Oil in Water AnalyzerModel 3.4.1.2Manual Mode Zeroing3-18Part 3 Operation3.4.1.3 Detector Failure Part IOil in Water Analyzer OperationHow the offset value is selected 3-20Part3 Operation ModelOil in Water Analyzer 3.4.2.1Auto Mode Spanning3.4.2.2Manual Mode Spanning Part IModel 3.5The Alarms Function3-22Part 3 OperationOperation Decide whether you want the alarms to be set asPart I Oil in Water AnalyzerModel 3.6The Range Select Function3-24Part 3 Operation3.6.1 Manual Select/Define Range Screen Part IOil in Water Analyzer OperationModel 3.6.3 Precautions3-26Part 3 OperationOperation 3.7The Analyze FunctionPart I Oil in Water AnalyzerModel 3.8Programming3-28Part 3 Operation3.8.1 The Set Range Screen Part IOil in Water Analyzer Operation3.8.2 The Curve Algorithm Screen 3-30Part3 Operation ModelOperation 3.8.2.2 Auto Mode LinearizationPart I Oil in Water AnalyzerTeledyne Analytical Instruments 3-32Part3 Operation ModelPart I: Maintenance4.1Fuse Replacement Maintenance4-2:Part 4.2System Self Diagnostic Test4 Maintenance PowerPart I: Control Section Maintenance4.3Major Internal Components Part I:4-4:Part Side ViewOpen Door 4 Maintenanceof the Control/Analysis Unit Part II: Analysis SectionModel Oil in Water Analyzerii: Part Table of ContentsInstallation MaintenanceTeledyne Analytical Instruments Part II:Part II: Analysis Unit Appendixiv: Part Model 6600 Oil in Water AnalyzerTeledyne Analytical Instruments Part II: Operational Theory1.0Introduction 1.1Method of AnalysisModel 1.2Optical Bench1-2Part 1 Operational TheoryOil in Water Analyzer Interconnection Diagram1.3Photometer Amplifier Part II:Model 1.4Automatic Zero System1-4Part 1 Operational TheoryOperational Theory 1.5System DescriptionPart II: Oil in Water AnalyzerModel 1.6Photometer1-6Part 1 Operational TheoryLOWED TO OPERATE UNLESS PERSONNEL IN Part II:Oil in Water Analyzer Operational TheoryModel 1.7Sample Systems1-8Part 1 Operational TheoryPart II: Installation2.2Installing and Connecting the Analyzer 2.1Unpacking the Analyzer2-2:Part 2 Installation2.2.2 Electrical Power Connections 2.2.5 Signal and Alarm Output ConnectionsOil in Water Analyzer 2.3Testing the System2.4Calibration 2.4.1 Calibration Fluids Part II:2.4.2 Calibration 2 Installation2-4:Part Model3.2System Visual Check and Response Procedure Maintenance3.0Routine Maintenance MaintenancePart 3 Maintenance3.3Routine Maintenance 3.4Suggested Preventive Maintenance SchedulePart Maintenance3.5Service Procedures and Adjustments 3.5.2 Power Supply Test PointsTeledyne Analytical Instruments 3 MaintenancePart ModelTeledyne Analytical Instruments MaintenancePart Oil in Water AnalyzerModel 3 Maintenance3.5.6 Setup of the Logarithmic Amplifier PartOil in Water Analyzer Maintenance3.5.8 Integrated Reference and Measuring Signals PartTeledyne Analytical Instruments 3 MaintenancePart ModelTeledyne Analytical Instruments MaintenancePart Oil in Water AnalyzerModel 3 Maintenance3-10 PartOPERATING INSTRUCTIONS Oil in Water Sample Conditioning System OperationPart III: Sample System ModelTeledyne Analytical Instruments Table of Contentsii: Part Model 6620 Oil in Water AnalyzerPart III: Part III: Oil in WaterTeledyne Analytical Instruments Teledyne Analytical Instruments iv: PartModel 6620 Oil in Water Analyzer 7.11Part 1.0IntroductionPart III: Oil in Water1-2Part 2.0The Method of Analysis2.1The Optical Bench 2.2The Photometer AmplifierThe detector output, which is a sequence of pulses which directly reflect the photo energy transmitted by the measuring and reference filter, is a measure of the concentration of the component of interest in the sample. The difference of the energy in the measuring and reference pulse is exponentially related to the concentration of the component of interest Part III:Oil in Water PartPart 2.4 From B71046-0or customer’s piping schematic2.3The Automatic Zero System 1-4PartPart Oil in Water Piping Diagram B71046Part III: Oil in WaterTeledyne Analytical Instruments 1-6PartPart ModelTOMER SPECIFIC PIPING Part III:Oil in Water PartModel 3.0System Description1-8Part PartPart III: 3.1Photometer3.1.1Source Module 3.1.2Sample CellModel 3.1.3Detector Module3.1.4Control/Analysis Unit PartPart III: 3.3Electrical Connections3.4The Sampling System 3.4.1Sample Water Preconditioning SystemCALIBRATION SAMPLE DELIVERY PartModel PRESSURIZED INLET SAMPLE DELIVERYPart III: Oil in Water Piping Diagram simplestHomogenizing 3.4.2Zero Water Preconditioning SystemModel 3.4.3The Automatic Sample Cell Cleaning Systemconfigured to measure non-dissolvedoil only PartEntering the zero offset Part III:Oil in Water PartModel 3.5The Signal Outputs3.6Recorder Requirement PartPart III: 3.7The Process Alarm System3.8The amplifier PCB 3.8.1Auto Zero CircuitModel 3.8.2 Signal Failure AlarmDetector Fail Check the Detector signal PartPart 4.0INSTALLATIONPart III: Oil in Water4.1.2Compressed Air Supply 4.1.1Electrical Power Connections4.1.4Signal and Alarm Output Connections 4.1User ConnectionsOil in Water 4.1.5 Sample Delivery System4.1.6Safe Vent Drainage Part III:Part 5.1Installation Check5.0SYSTEM START-UP/CALIBRATION 5.2Electronics CheckPart III: 5.3Electrical Check5.4Sample Delivery Check 5.5Preparation for CalibrationManual Sample Introduction 5.5.1Required Calibration EquipmentPart ModelOil in Water 5.5.2Acquisition of Representative Oil Sample5.5.3Acquisition of Representative Sample Water Part III:1-26Part III Teledyne Analytical Instruments 5.5.5Background Signal Level DeterminationPart ModelInterpretation of Observations Part III:Oil in Water PartPart Model1-28Part III Teledyne Analytical Instruments Part III: 5.6Calibration with Prepared Sample5.6.1Zero Fluid Preparation 5.6.2Span Fluid Preparation1-30Part III Teledyne Analytical Instruments 5.6.3 CalibrationPart ModelPart Setup of Internal Span Flag CalibrationPart III: Oil in WaterSample System PartModel SpanFilter6.Analyze both samples in the laboratory Part III:Oil in Water Part1-34Part III Teledyne Analytical Instruments 5.6.5Calibration of the ultrasonic homogenizerPart Model5.7.1Set-upfor Automatic Sampling HomogenizerTuningCORRELATION 5.7System Set-UpFor Automatic Operation1-36Part III Teledyne Analytical Instruments 5.7.2Electronics Set-upfor Automatic OperationPart ModelOil in Water 6.1System Visual Check and Response Procedure6.2Routine Maintenance Part III:WEEKLY PartModel DAILYPart 7.0SERVICE PROCEDURES AND ADJUSTMENTSPart III: Oil in Water1-40Part III Teledyne Analytical Instruments 7.2Set Up of the I to E ConverterPart ModelPart III: 7.3Set Up of the Logarithmic Amplifier7.5The Integrated Reference and Measuring Signals 7.4The Inverting AmplifierCAUTION: wear UV goggles if lamp left on 7.6Sample Cell MaintenancePart ModelOil in Water 7.7Sample System Maintenance7.8Zero Filter Replacement Part III:1-44Part III Teledyne Analytical Instruments 7.9316 Zero Filter Cleaning ProcedurePart Model7.11 7.10 Lamp ReplacementPhototube Replacement PROCEDURE8.2.1The Water Refuses to Flow Through the Tubing 8.0TROUBLESHOOTING SECTION8.2Water Delivery Problems 8.1The Lamp Refuses to LightOil in Water 8.3Zero Drift Problems8.2.2Sample Pump Failure Part III:Part CommissioningandStart-upGuide for Oil in Water Analyzer Systems A Site requirements1 Electrical connections B Installationapower 3Sample Connections 4 See section for the Alarms Functionc DCS connections 1Please refer to Section 1.5 Control Unitsee addendum drawings drawingsB Start up of System aPiping Diagram, see addendum drawingsbOutline drawing see addendum drawings Part III:7 Once assured sample inlet is proceed as follows Oil in Water E Set up of internal calibration span flagFSet up for Automatic Sampling Sample System Part III:Automatic Operation and Routine Duties PartModel 1-56Part III Teledyne Analytical InstrumentsTeledyne Analytical Instruments Part III:Oil in Water Part6600 Digital Control Module AppendixA-1Specifications Operating Temperature: 0-50oCModels Typical Analytical Performance SpecificationsSample temperature AppendixAppendix A-2Recommended 2-YearSpare Parts ListModel Oil in Water AnalyzerModels A-3Drawing List See manual addendumGeneric Drawing List Appendix