M9110T Date 11/15/13
Teledyne Electronic Technologies
Copyright 2013 Teledyne Analytical Instruments
Model 9110T NOx Analyzer
Model 9110T- Standard Touch Screen Version
Model 9110TH NOx Analyzer Specific Configuration
Rear Panel Gas Fittings
Model 9110T NOx AnalyzerSpecific Configuration
Mounting Options
Pump Mounting Options
Background Gas
This option includes two concentration alarm relays
Model 9110T NOx Analyzer Specific Configuration
Or by accessing various service options on our website at
Safety Messages
Model 9110TH NOx Analyzer Safety Messages
Customer Service Department
Model 9110T NOx Analyzer Safety Messages
Consignes DE Sécurité
Mise EN Garde
Organization
Instrument and possibly invalidate the warranty
Maintenance of the analyzer or its parts
About this Manual
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Table of Contents
Model 9110T NOx Analyzer Table of Contents
Model 9110TH NOx Analyzer Table of Contents
285
Appendix a Version Specific Software Documentation
Figures
229
Ventilation Clearance
Tables
325
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Model 9110TH NOx Analyzer Part
Part General Information
Model 9110T NOx Analyzer Part
Features
Overview
Model 9110TH NOx Analyzer Introduction
Analyzer Options Description/Notes Reference Number
Documentation
Options
Model 9110T NOx Analyzer Introduction
Ambient Zero and Pressurized Span Valves
Option Description/Notes Reference Number
9110T Analyzer Weighs about 18 KG 40 Pounds
Ambient Zero and Ambient Span Valves
USB Port For remote connection
Specifications
9110T Basic Unit Specifications Parameter
Specification
Parameter Specification
Software Settings for EPA Equivalence Parameter
EPA Equivalency Designation
North American
Approvals and Certifications
Other Type Certifications
Calibration
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Model 9110TH NOx Analyzer Getting Started
Instrument warranty. Refer to for more information on
Under Customer Support Return Authorization
Unpacking the 9110T Analyzer
10 cm / 4
Instrument Layout
Ventilation Clearance
Model 9110T NOx Analyzer Getting Started
Front Panel Layout
Front Panel
Display Screen and Touch Control
Buttons
Field Description/Function
Display Screen and Touch Control Description
Actual display
Provides a description of each component on the rear panel
Rear Panel
Internal Chassis Layout
Internal Layout Top View with IZS Option
Internal Layout Top View Showing Other Options
Electrical Connections
Connections and Setup
Connecting Power
Connecting Analog Inputs Option
Connecting Analog Outputs
Analog Input Pin Assignments
PIN Description DAS Parameter
Test Channel
Current Loop Analog Outputs Option 41 Setup
Current Loop Option Installed on the Motherboard
10 Status Output Connector Status Output Pin Assignments
Connecting the Status Outputs
On Condition
Connecting the Control Inputs
Diag Mode
Input #
Concentration Alarm Relay Option
Alarm 1 Relay
Alarm 2 Relay & Alarm 3 Relay
Alarm 4 Relay
Connecting the Communications Interfaces
Anything other than Multidrop communication
Configuration Section
Before using
Communication
13 Rear Panel Connector Pin-Outs for RS-232 Mode
Using
RS-485 operation
∙ Parity None
RS-232 Multidrop Option 62 Connection
15 Jumper and Cables for Multidrop Mode
Time, each by its unique ID see above
Host
Analyzer
Last Analyzer
Testing it before setting up the rest of the chain
Pneumatic Connections
RS-485 Connection
Cc3/min x
Been made check all pneumatic fittings for leaks using
Procedures defined in Section
About Zero Air and Calibration Span Gas
NIST-SRM Type Nominal Concentration
Cylinders
Available
Calibration Span GAS
Span GAS for Multipoint Calibration
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Connect a sample gas line to the Sample inlet
Sample GAS Source
Calibration GAS Sources
Exhaust Outlet
Pneumatic Layout for Basic Configuration
13.3.13.2 or 13.3.13.3 for detailed check if leak suspected
Venting
This valve package includes
19 Pneumatics, Basic Configuration
20 Rear Panel Layout with Z/S Valve Options OPT 50A
Attach a sample inlet line to the Sample inlet fitting
13.3.12
Mode Valve Condition Valve Port Status Sample
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Attach a line to the SPAN2/VENT outlet. It should be
Pneumatic Layout for Ambient ZERO/PRESSURIZED Span OPT 50B
10 Valve Operating States OPT 50B installed
Mode Valve Condition Valve Port Status
Zero Scrubber and Internal Span Source IZS OPT 50G
Nitric Acid and the Chemistry of NO2 Permeation Tubes
Internal Span GAS Generation
Pneumatic Layout for Zero Scrubber and IZS OPT 50G
Gas Conditioner Options
Ammonia Removal Sample Conditioner OPT 86A
Zero AIR Scrubber OPT 86C, for Z/S Valves
Model 9110TH NOx Analyzer Getting Started
Start UP
STARTUP, Functional CHECKS, and Initial Calibration
Model 9110TH NOx Analyzer Getting Started
12 Possible Warning Messages at Start-Up
Initial Calibration
Functional Checks
Following procedure assumes that
Interferents for NOX, no and NO2 Measurements
Calibration on the analyzer
Verifying the Reporting Range Settings
Verifying the Expected NOX and no Span GAS Concentration
Verify the Precise Concentration Value of the Span gases
Independently
No x Must be identical
Model 9110TH NOx Analyzer Getting Started
Initial ZERO/SPAN Calibration Procedure
Improving our service and our products. Thank YOU
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Page
Part Operating Instructions
Model 9110T NOx Analyzer Part
An allowable value, the Entr button will re-appear
Model 9110TH NOx Analyzer Overview of Operating Modes
Analyzer Operating Modes
Sample Mode
Test Functions
Model 9110T NOx Analyzer Overview of Operating Modes
Samp
To view these Test functions, press
Viewing 9110T Test Functions
Absolute atmospheric pressure
System Reset
Cannot DYN Span
Cannot DYN Zero
Setup Mode
Calibration Mode
Primary Setup Mode Features and Functions
Password Security
Primary Setup Menu
Secondary Setup Menu Setup MORE
Entered value had not been accepted
Model 9110TH NOx Analyzer Setup Menu
Setup CFG Configuration Information
Setup ACAL Automatic Calibration Option
Setup DAS Internal Data Acquisition System
Analog Output Reporting Ranges
Setup RNGE Analog Output Reporting Range Configuration
Model 9110T NOx Analyzer Setup Menu
Physical Ranges
When switching between reporting range modes, Always check
Analog OUT
For the other modes
Reset the upper range limits for the new mode selection
Analog Output Reporting Range Default Settings
IND Mode Analog Output Assignments
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High physical ranges referred to in Section
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Importantimpact on Readings or Data
Setup Rnge DIL Using the Optional Dilution Ratio Feature
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Password Level
Setup Pass Password Protection
To enable passwords, press
Password Levels
Has to press Entr to access the password-protected menus
Setting the Time of DAY
Setup CLK Setting the Internal TIME-OF-DAY Clock
Adjusting the Internal CLOCK’S Speed
ID Machine Identification
Setup Comm Communications Ports
COM1COM2 MODE, Baude Rate and Test Port
Setup Vars Variables Setup and Definition
Use the SETUPCOMMCOM1COM2 menus to
Inet Ethernet
Allowed Vars Variable Description Default Values
OFF
Auto
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Setup Diag Diagnostics Functions
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Stsystemok = on
STSYSTEMOK=ON
Analog Output Diag Aout
Analog I/O Configuration Diag AIO
Accessing the Analog I/O Configuration Submenus
To access the Analog I/O Configuration sub menu, press
Analog Output Voltage Range Min/Max
Range Name Range Span Minimum Output Maximum Output
Curr
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Automatic Individual Calibration of the Analog Outputs
Analog output is enabled. See Section
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Adjusted. See Section
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Current Loop Output Check
Turning AN Analog Output OVER-RANGE Feature ON/OFF
Adding a Recorder Offset to AN Analog Output
Model 9110TH NOx Analyzer Setup Menu AIN Calibration
SET Exit
External Analog Inputs XIN1…XIN8 Option Configuration
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Test functions available to be reported are listed in Table
To activate the Test Channel and select a function, press
Optic Test
Changes with low-level calibration
Electrical Test
Ozone GEN Override
Flow Calibration
MODE1
Communication MODES, Baud Rate and Port Testing
Data Terminal / Communication Equipment DTE DEC
Communication Modes
Model 9110T NOx Analyzer Communications Setup and Operation
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COM Port Baud Rate
COM Port Testing
Communications Menu
Sample RANGE=500.0 PPB NOX= TST TST CAL Setup
Setup X.X Primary Setup Menu
Secondary Setup Menu Comm Vars
LED Function
To configure Ethernet communication manually
Ethernet Status Indicators
Ethernet
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Default Ethernet setting is Dhcp
Access the Communications Menu SETUPMORECOMM, see
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USB Port for Remote Access
Baud Rate COM2 Mode Settings Quiet Mode Computer Mode
1 Mode
PC match check the PC baud rate and change if needed
Communications Protocols
Minimum Requirements
Actions
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Properly set
RS-232 Communication Parameters for Hessen Protocol
Parameter Standard Hessen
Activating Hessen Protocol
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BCC
Mode ID Mode Description CMD
To select a Hessen Protocol Type press
To Select a Hessen response mode, press
GAS TYPE,RANGE,GAS ID,REPORTED
Hessen Protocol GAS List Entry Format and Definitions
NO, 0, 212, Reported NO2, 0, 213, Reported
To add or edit an entry to the Hessen Gas List, press
Editing or Adding Hessen GAS List Entries
Deleting Hessen GAS List Entries
To delete an entry from the Hessen Gas list, press
Setting Hessen Protocol Status Flags
Unassigned Flags
Default Hessen Status Flag Assignments
Status Flag NAME3 Default BIT Assignment
Operational Flags
Instrument ID
To assign or reset the status flag bit assignments, press
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LED State
There is reset
Front Panel LED Status Indicators for DAS
Interface for DAS changes Section
DAS Structure
DAS Channels
Channels
CAL Hold OFF
Default DAS Channels
Property Description Default Setting Range Channel
Enabled
Settings
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DAS View Touchscreen Functions Button
Viewing DAS Data and Settings
Editing DAS Data Channels
Translates to the following configuration
NXCNC1 ATIMER, 5
Name NXCNC1 Trigger Event Atimer
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Manual
DAS Data Parameter Functions
Changed during data acquisition
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AVG, SDEV, MIN or MAX sample modes see .1.3.3,
Stored and reported to the Comm ports
Report period
Report Periods in Progress when Instrument Is Powered Off
Editing the Number of Records
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ON/OFF
Holdoff Feature
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Disabling/Enabling Data Channels
Starting Date Feature
DAS Configuration VIA Apicom
Remote DAS Configuration
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DAS Configuration VIA Terminal Emulation Programs
Whereas the editing, adding and deleting of DAS channels
Advised before attempting any DAS changes
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Remote Control VIA a Terminal Emulation Program
Computer Mode
Interactive Mode
Remote Control VIA Apicom
Where
Command Syntax
Terminal Mode Software Commands
Command Command Type
Data Types
Status Reporting
General Message Format
Remote Access by Modem
Model 9110T NOx Analyzer Remote Operation
AT Y0 D0 H0 I0 S0=0
To initialize the modem press
Remote Access by Modem
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Where N is any numeral between 0
Password Security for Serial Remote Communications
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Calibration Quality Analysis
Model 9110TH NOx Analyzer Calibration Procedures
Model 9110T NOx Analyzer Calibration Procedures
Before Calibration
Required EQUIPMENT, SUPPLIES, and Expendables
Example
Calibration Gases
Zero Air
Span Gas
Measured medium as closely as possible
Data Recording Devices
Span Gas for Multipoint Calibration
2.4. NO2 Permeation Tubes
ZERO/SPAN Calibration Checks VS. ZERO/SPAN Calibration
4. NO2 Conversion Efficiency CE
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Outside the allowable range for a reliable calibration
See for troubleshooting tips
Performing a Basic Manual Calibration Check
Performing a Basic Manual Calibration
Entered properly in the conversion efficiency setting
Setting the Expected Span Gas Concentration
For troubleshooting tips
As a calibration source
Manual Calibration with the Internal Span GAS Generator
Setup for Calibration with the Internal Span GAS Generator
CAL on NO2 Feature
Check is performed
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Troubleshooting tips
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Calibration. See for troubleshooting tips
Setup for Calibration Using Valve Options
Sample TST TST CAL Cals Setup
Manual Calibration Checks with Valve Options Installed
Manual Calibration Using Valve Options
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Autocal Modes
Mode Name Action
Disabled
Automatic ZERO/SPAN CAL/CHECK Autocal
Analyzer’s sample port
AutoCal Attribute Setup Parameters
For US EPA controlled/related applications
Always be set to OFF
0030
Sept
100 AM
15.0
To program the example sequence shown in -4, press
Setup Acal Programming and Auto CAL Sequence
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Entr button will disappear from the display
No Offs No Slope NOX Offs NOX Slope
Calibration Quality Analysis
GAS Flow Calibration
Separate flow meter is required for this procedure
Model 9110T NOx Analyzer EPA Protocol Calibration
Calibration General Guidelines
Spare Parts and Expendable Supplies
Calibration EQUIPMENT, SUPPLIES, and Expendables
Record Keeping
Calibration Frequency
Calibration GAS and Zero AIR Sources
Data Recording Device
Definition of Level 1 and Level 2 Zero and Span Checks
Level 1 Calibrations Versus Level 2 Checks
Equation
GAS Phase Titration GPT
GPT Calibrator Check Procedure
GPT Principle of Operation
≤ 2min
Have to be made, and TR and PR will have to be recalculated
Example GPT Calculation
GPT Multipoint Calibration Procedure
Conditions of use against a reliable standard
Handbook, Vol. II, Part 1, Appendix
GPT Calibration System
SET UP for GPT Multipoint Calibration of the 9110T
Span Calibration
Zero Calibration
GPT NO2 Check
See the Troubleshooting if there are problems
Summary of Quality Assurance Checks
Other Quality Assurance Procedures
Short Calibration Checks
ZERO/SPAN Check Procedures
Precision Check Procedure
Certification of Working Standards
Precision Check
Standard
Certification Procedures of Working Standards
References
Other Methods of Establishing Traceability
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Part Maintenance and Service
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Model 9110T NOx Analyzer Instrument Maintenance
Maintenance Schedule
CAL Date Performed Action Freq Check REQ’D
9110T Maintenance Schedule
Function Expected Actual Interpretation & Action
Predictive Diagnostics
Maintenance Procedures
Predictive Uses for Test Functions
Replacing the Particulate Filter
Replacing the Sample Particulate Filter
Turn against the Perma Pure dryer
Risk of causing a significant leak
Changing the O3 Dryer Particulate Filter
Ensure to use proper wrenches
Changing the Ozone Cleanser Chemical
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Offsets, which may take 2-3 weeks to disappear
Replacing the Scrubber
Maintaining the External Sample Pump Pump Pack
Changing the Pump DFU Filter
Rebuilding the Pump
Procedure for Replacing Filters on Internal Pumps
Procedure for Replacing Filters on External Pumps
Room temperature and will contaminate the entire instrument
Changing the Internal Span GAS Generator Permeation Tube
Changing the External Zero AIR Scrubber OPT 86C
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Changing the External Scrubber’s DFU Filter
Zero Air Scrubber Assembly
HOT Surface Hazard
Changing the NO2 Converter
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Cleaning the Reaction Cell
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Replacing Critical Flow Orifices
To clean or replace a critical flow orifice
From the vacuum port to get the parts out of the manifold
Checking for Light Leaks
Assembly
Checking for Pneumatic Leaks
Simple Vacuum Leak and Pump Check
Surfaces
Detailed Pressure Leak Check
Performing a Sample Flow Check
Instrument
This value is only calculated, not measured
Model 9110T NOx Analyzer Troubleshooting & Service
General Troubleshooting
Fault Diagnosis with Warning Messages
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Front Panel Warning Messages
XXX.X MV
Ozone Flow
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Can also cause changes in the absolute atmospheric pressure
Fault Diagnosis with Test Functions
OUT of Range reading
Pressure
Indicated Failures
Diag Signal I/O Using the Diagnostic Signal I/O Function
Under this menu
These signals upon exit
Test Channel Outputs as Diagnostic Tools
Using the Analog Output Test Channel
12.3.2.1. I2C Bus Watchdog Status LEDs
Using the Internal Electronic Status Leds
CPU Status Indicator
Relay PCA Status Leds
Relay PCA Status LED Failure Indications
LED Color Function Fault Indicated Failures Status LED ROW
D10 Green NO/NOx Valve D9 Green AutoZero Valve
D1 RED
About 1 in-Hg per 300 m / 1000 ft
GAS Flow Problems
Zero or LOW Flow Problems
Sample Flow is Zero or Low
Ozone Flow is Zero or Low
Check pressures
High Flow
Check if the particle filter is clogged
Sample Flow is Zero or Low but Analyzer Reports Correct Flow
Negative Concentrations
Calibration Problems
Unstable Zero and Span
No Response
Inability to Zero no Zero Button Calz
Inability to Span no Span Button Cals
NON-LINEAR Response
Discrepancy Between no and NOX Slopes
Discrepancy Between Analog Output and Display
Other Performance Problems
Excessive Noise
Slow Response
Dirty reaction cell can cause high Auto Zero values
Auto Zero Warnings
AC Main Power
DC Power Supply
Subsystem Checkout
DC Power Test Point and Wiring Color Codes
DC Power Supply Acceptable Levels
From
Touchscreen Interface
LCD/DISPLAY Module
Motherboard
Test Channel / Analog Outputs Voltage
Step Nominal Output Voltage
12.7.6.2. A/D Functions
Analog Output Test Function Nominal Values Voltage Outputs
Full Scale Output of Voltage Range
Status Outputs
To test the status output electronics
Ozoneflow
10 Status Outputs Check
Control Inputs
Pressure / Flow Sensor Assembly
Basic PCA Operation Check
Sample Pressure Sensor Check
12.7.7.4. O3 Flow Sensor Check
General RS-232 Troubleshooting
RS-232 Communications
Vacuum Pressure Sensor Check
RS-232 Programming Notes TAI P/N
Troubleshooting Analyzer/Modem or Terminal Operation
Doubt, consult the factory
12.7.10.1. NO2 no Converter Electrical System
Calculating / Checking Converter Efficiency
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Step
Evaluating NO2 no Converter Performance
Simplified GPT Calibration
Concentration must be used must be 440 ppb or more
There must be a minimum of 10% more no than O3 produced
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NOx Loss
OUT-GASSING no NOX
Photomultiplier Tube PMT Sensor Module
Optic Test
To activate the optics test, press
To activate the electrical test, press
PMT Preamplifier Board
High Voltage Power Supply
PMT Temperature Control PCA
12.7.15.1. O3 Generator Override
12.7.15. O3 Generator
Exit the menu
Internal Span GAS Generator and Valve Options
Temperature Sensor
Box Temperature Sensor
PMT Temperature Sensor Control
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Expendables are discussed in Instrument Maintenance
Service Procedures
DISK-ON-MODULE Replacement Procedure
Procedures. Contact Teledyne Customer Service Department
12.8.2. O3 Generator Replacement
Sample and Ozone Perma Pure Dryer Replacement
Analyzer has warmed up for about 60 minutes
To calibrate the PMT preamplifier PCA
PMT Sensor Hardware Calibration
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Replacing the PMT, Hvps or TEC
Between measure and Auto Zero modes
Qualified Personnel
9110T Sensor Assembly
Ensure to replace the 5 desiccant bags inside the housing
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10 Relay PCA with AC Relay Retainer In Place
Removing / Replacing the Relay PCA from the Instrument
Frequently Asked Questions
Question
Answer
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Analytical Instruments
Technical Assistance
Measurement Principle
Chemiluminescence Creation in the 9110T Reaction Cell
Model 9110T NOx Analyzer Principles of Operation
NO2* →NO2 + hν1200nm
Chemiluminescence Detection in the 9110T Reaction Cell
Photo Multiplier Tube PMT
Optical Filter
Tensit
NOX and NO2 Determination
XNO2 + yMo→ xNO + MyOz at 315C
Direct Interference
Measurement Interferences
Light Leaks
Reaction Cell Temperature Control
List of Interferents
Gas Interference Type Rejection Method
Zero a perfect vacuum
Pneumatic Operation
Sample GAS Flow
Both leak tight and not pressurized over ambient pressure
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Basic Internal Gas Flow for Basic 9110T with Internal Pump
Vacuum Manifold
9110T Valve Cycle Phases
Sample Gas Flow Valves and Routing
NO/ no
Critical Flow Orifice
Flow Rate Control Critical Flow Orifices
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Maintained at a constant temperature
Ozone GAS Generation and AIR Flow
O3 Generator
10 Ozone Generator Principle
Ozone Generator Dry Air Supply
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Down, the generator is turned on immediately
Pneumatic Sensors
Ozone Supply Air Filter
Ozone Destruct
Samplepressure
Sample Pressure Sensor
Vacuum Pressure Sensor
Sample Gas Flow Calculation
13.2.4.4. O3 Supply Air Flow Sensor
Electronic Operation
13 9110T Electronic Block Diagram
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Flash Chip
Disk-On-Module
Sensor Inputs
Thermistor Interface
Reported nor stored
Analog Outputs
External Digital I/O
Motherboard see Section
13.3.3.7. I2C Data Bus
Only until signal I/O menu is exited
To their normal value/setting
Internal Digital I/O
Electrical Shock Hazard
15 Relay PCA Layout P/N
16 Relay PCA P/N 045230100 with AC Relay Retainer in Place
Status LED’s
Relay PCA Status LED’s
Color Function Status When Lit Status When Unlit
Watchdog Circuitry
Valve Control
Yellow no 2 no Converter Heater
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TC1
TC1
Sensor MODULE, Reaction Cell
TC2
Not Used
Photo Multiplier Tube PMT
20 9110T Sensor Module Assembly
PMT preamplifier board provides a variety of functions
PMT Preamplifier
Principles of Operation
22 PMT Preamp Block Diagram
23 Typical Thermo-Electric Cooler
PMT Cooling System
Preamp
Pneumatic Sensor Board
TEC Control Board
PMT
All AC and DC Voltages are distributed via the relay PCA
Power SUPPLY/CIRCUIT Breaker
Logic Devices
AC Power Configuration
Sensor Module
Hvps PMT
Configuration Jumpers for Optional AC Heaters
Pump Configuration
Configuration Jumpers For AC Heaters
AC Power Configuration for Internal Pumps JP7
White
AC Configuration Heaters for Option Packages JP6
Power Configuration for Standard AC Heaters JP2
VAC /115 VAC VAC / 240 VAC
IZS
Power Configuration for Optional Heaters JP6
Jumper Heaters Between Function Color Pins
RED
Front Panel TOUCHSCREEN/DISPLAY Interface
30 Front Panel and Display Interface Block Diagram
Software Operation
Lvds Transmitter Board
Front Panel TOUCHSCREEN/DISPLAY Interface PCA
TEMPERATURE/PRESSURE Compensation TPC
Adaptive Filter
Calibration Slope and Offset
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Means of Generation
HOW Static Charges are Created
Model 9110T NOx Analyzer Primer on ESD
Static Generation Voltages for Typical Activities
Damage Susceptibility Voltage
HOW ELECTRO-STATIC Charges Cause Damage
Potentially damaging electro-static discharges can occur
Sensitivity of Electronic Devices to Damage by ESD
Common Myths about ESD Damage
Basic Principles of Static Control
General Rules
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Working AT AN ANTI-ESD Work Bench
Working AT the Instrument Rack
Transferring Components Between Rack and Bench
Opening Shipments from TAI Customer Service
ESD Hazard
Packing Components for Return to TAI Customer Service
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Glossary
Model 9110T NOx Analyzer Glossary
Term Description/Definition
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